Right..here we are..
Now I'm on my 3rd week after returning from my hometown..
For last 2 weeks..coping with jet lag..the annual review presentation.I must say..life goes on...it's not easy to get back to the mood..but this laziness must be fought...I must..I shouldn't waste my time..
So to start off the 2nd year...I've open a new logbook..for 2nd year..since there're only several pages left..well this is a good sign and a good start isn't it??To start a new book for a new year!What a timing!!
Besides, since last week I took a text books on thermodynamic and chemisty which I've loaned many2 weeks ago, laid neatly on my desk..'trying' to finish some chapters on chemical metallurgy..and there the literature writing again...
And so this week..I'm stuck with another 2-3 books I've loaned...and hopefully I'll have my full mood, spirit and strength to at least understand all the related topic more clearly..to get clearer fundamental knowledge of thermochemistry, reaction kinetics, mineral separation, metal extraction..refining...and the lists goes...argh...!!but i must..the target???regard them as novels of my fav authors, I should finish 'extract' and 'absorb' the story in the book at the end of next week.And so.. for next term...I'm planning to join the thermodynamic lectures of Tony and Keith, so that I'll get better picture of the subjects..which I've never learn before..
Eventhough it's hard..having all the comments and recommendation from the annual review presentation session, I should appreciate as now I got clearer focus and direction to begin my 2nd year...
But hang on..today I'm going to start by reviewing my 1st year log book at least for once..to refresh!
End.
Anything...everything associates, relates, link to this PhD phase.. Including some technical infos on research title itself : Valuable Metal Recovery from Steelmaking Waste
Tuesday, April 27, 2010
Wednesday, April 21, 2010
Comments and notes from 1st Year VIVA
Annual Review Presentation
Day/Date : Tuesday, 20th April 2010
Day/Date : Tuesday, 20th April 2010
Time : 2.05 - 2.50 p.m.
Venue : Tony's room
Examinars : Tony, Keith, Devin
1) Need to adjust and prioritize in the research aim. You've shown many works on the extraction process..but your aim stated about environmental management as first aim..which one's first?
- Extraction and recovery. The environmental management is by product of the outcome. Through out the process, the environmental management might as well will not be a priority. So..just focus on the metal extraction and recovery process...so the aim of the research will just be on the extraction and recovery mechanism!They asked : Are u okay and comfortable with that??Yes!Better where I'll just have to focus on one aim then!Eventhough the subject is hard, I love what I'm doing!
2) Have u checked on the latest updates and amendment if any for the waste disposal compliance?Fuh...
- Nope!I misssed that one!I have no answer for that one!I should if I supposed to checked on the environmental management point of view..all this while I've been worrying and working so hard on the extraction mechanism..(which because I have no fundamental background on thermodynamic...phase reaction..all those solid state and inorganic chemistry!Fuh!)
3) What's the different of all the heterogenous materials on the waste you're working on?Are they no different?Are they from the same sources?You need to have more infos and details on the production line that produced the heterogeneous materials on the waste u're working on. Need to work close to Julian and Martyn to find the answer.
- Yes..my fault..I need to put more indepth on that one..will do!
4) What's the value of the recovered material that u intend to extract to the company?
- Argh!!!!!I just can't remember the figure!!!!How many millions per tonne??I should know this at my finger tips!?It's 23 milion for Zinc and 31 millions for Iron!
5) Why Chloride Extraction?What's with other mechanism?Sulphatization perhaps??
- Easier to extract metal in chloride form rather than oxides. Sulphatization is common but it could assist in the chloride extraction anyway. I had explain the results of the works carried out by Mike, the engineer who run the experiment using my sample..and the results from my own experiments as well..the results were outstanding...so that the process will have a very big potential to be examined further..but as the experiments only ran with one duration and temperature, now my plan is to study the factors of gradual duration, gradual temperature and chemical :sample ratio towards rate of reaction and so the next step would be to recover the metal.
6) The chemical agent you're using now is quite expensive.Have u ever tried and consider using other chemicals?Compare the outcome?
-Well..it's quite hard to find the extraction using the chemical I'm using now from literatures...and dealing with heterogenous materials not single source as most of the literatures stated, so I believed the novelty is there..I've considered other chemicals..and different roasting process and mechanism as well..but as the previous works proven the high percentage of exttraction, so I thought, this is great..I shall proceed...adding the factors and parameters..but I'll do...try on other chemical as well!and compare!
Okay..now obtaining clearer direction of my research..I shall proceed and more focus!I'll be okay!
End.
5) Why Chloride Extraction?What's with other mechanism?Sulphatization perhaps??
- Easier to extract metal in chloride form rather than oxides. Sulphatization is common but it could assist in the chloride extraction anyway. I had explain the results of the works carried out by Mike, the engineer who run the experiment using my sample..and the results from my own experiments as well..the results were outstanding...so that the process will have a very big potential to be examined further..but as the experiments only ran with one duration and temperature, now my plan is to study the factors of gradual duration, gradual temperature and chemical :sample ratio towards rate of reaction and so the next step would be to recover the metal.
6) The chemical agent you're using now is quite expensive.Have u ever tried and consider using other chemicals?Compare the outcome?
-Well..it's quite hard to find the extraction using the chemical I'm using now from literatures...and dealing with heterogenous materials not single source as most of the literatures stated, so I believed the novelty is there..I've considered other chemicals..and different roasting process and mechanism as well..but as the previous works proven the high percentage of exttraction, so I thought, this is great..I shall proceed...adding the factors and parameters..but I'll do...try on other chemical as well!and compare!
Okay..now obtaining clearer direction of my research..I shall proceed and more focus!I'll be okay!
End.
Thursday, April 15, 2010
Annual review aka 1st year viva
After 3 days returned from hometown, I was informed by Tony that my annual review aka 1st year viva will be held next week, Tuesday afternoon...As I've completed the annual review forms and report before I went back for the 5 weeks break and while I was away Tony has filled in the forms and submitted the to the Research Office..no wonder the date is due this soon!Tony told me there's nothing to worry, just compile and summarise all the presentations I've made thru last 11 months, mention all the works I've done to date and put one additional slide for future plan..Phew!!!!!
Well..the compilation is really not a problem..but the xtra reading will be through this weekend!!!!!!The scariest thing : Q & A !!I 've 4 days to prepare myself!!
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